Structures by: Ionkin A. S.
Total: 116
C11H20O2
C11H20O2
Organic letters (2008) 10, 11 2303-2305
a=7.166(3)Å b=18.830(9)Å c=8.506(4)Å
α=90.00° β=99.818(9)° γ=90.00°
C11H20O2
C11H20O2
Organic letters (2008) 10, 11 2303-2305
a=6.752(3)Å b=10.198(5)Å c=17.425(9)Å
α=90.00° β=90.00° γ=90.00°
C28H56O2P2Si2
C28H56O2P2Si2
Dalton Transactions (2009) 47 10574-10580
a=17.239(9)Å b=9.498(5)Å c=21.389(11)Å
α=90.00° β=99.493(8)° γ=90.00°
C22H40O2P2
C22H40O2P2
Dalton Transactions (2009) 47 10574-10580
a=24.140(12)Å b=8.856(5)Å c=11.564(6)Å
α=90.00° β=109.681(8)° γ=90.00°
C28H56O2P2Si2
C28H56O2P2Si2
Dalton Transactions (2009) 47 10574-10580
a=17.1720(18)Å b=17.1720(18)Å c=60.643(7)Å
α=90.00° β=90.00° γ=120.00°
C13H24CsO2P
C13H24CsO2P
Dalton Transactions (2009) 47 10574-10580
a=5.9871(4)Å b=9.5553(7)Å c=14.2529(10)Å
α=80.3510(10)° β=82.1280(10)° γ=81.0320(10)°
C34H12Ag3F27N2O6
C34H12Ag3F27N2O6
Dalton transactions (Cambridge, England : 2003) (2006) 20 2468-2478
a=8.2935(15)Å b=12.797(2)Å c=19.913(3)Å
α=82.984(3)° β=83.660(3)° γ=83.647(3)°
C61H31F36IrN4
C61H31F36IrN4
Dalton transactions (Cambridge, England : 2003) (2006) 20 2468-2478
a=12.9220(13)Å b=15.9360(16)Å c=17.7587(18)Å
α=67.8845(17)° β=72.2741(17)° γ=69.862(2)°
C28H10F18N2
C28H10F18N2
Dalton transactions (Cambridge, England : 2003) (2006) 20 2468-2478
a=10.4708(12)Å b=11.8225(14)Å c=12.6383(15)Å
α=104.597(2)° β=105.654(2)° γ=105.656(2)°
C42H15F27IrN3
C42H15F27IrN3
Dalton transactions (Cambridge, England : 2003) (2006) 20 2468-2478
a=41.862(4)Å b=9.2252(9)Å c=22.004(2)Å
α=90.00° β=99.2780(18)° γ=90.00°
C39H29F18IrN2O2
C39H29F18IrN2O2
Dalton transactions (Cambridge, England : 2003) (2006) 20 2468-2478
a=20.852(4)Å b=16.227(3)Å c=24.092(4)Å
α=90.00° β=90.00° γ=90.00°
C34H30F18IrN2O12P3
C34H30F18IrN2O12P3
Dalton transactions (Cambridge, England : 2003) (2006) 20 2468-2478
a=10.923(6)Å b=14.898(8)Å c=15.863(8)Å
α=64.147(8)° β=85.432(9)° γ=85.384(9)°
C11H21O2P
C11H21O2P
Chemical communications (Cambridge, England) (2008) 42 5432-5434
a=6.1970(4)Å b=8.5935(5)Å c=11.9624(7)Å
α=79.0472(10)° β=85.1087(11)° γ=80.2040(10)°
C28H56O2P2Si2
C28H56O2P2Si2
Chemical communications (Cambridge, England) (2008) 42 5432-5434
a=17.1720(18)Å b=17.1720(18)Å c=60.643(7)Å
α=90.00° β=90.00° γ=120.00°
C22H39O2P
C22H39O2P
Chemical communications (Cambridge, England) (2008) 42 5432-5434
a=11.3952(6)Å b=11.9039(6)Å c=33.5993(17)Å
α=90.00° β=90.00° γ=90.00°
C22H39O3P
C22H39O3P
Chemical communications (Cambridge, England) (2008) 42 5432-5434
a=44.018(15)Å b=9.170(3)Å c=23.309(8)Å
α=90.00° β=90.00° γ=90.00°
C58H60
C58H60
Chemical communications (Cambridge, England) (2008) 20 2319-2321
a=15.3050(15)Å b=9.6769(9)Å c=14.6721(15)Å
α=90.00° β=90.280(2)° γ=90.00°
C42H67F2NSi3
C42H67F2NSi3
Organometallics (2003) 22, 20 4136-4144
a=15.9934(9)Å b=23.5445(12)Å c=11.4333(6)Å
α=90.0000(10)° β=90.0000(10)° γ=90.0000(10)°
C30H43F2NSi3
C30H43F2NSi3
Organometallics (2003) 22, 20 4136-4144
a=18.916(3)Å b=19.462(2)Å c=34.126(5)Å
α=90.0000(10)° β=90.0000(10)° γ=90.0000(10)°
C18H29F3Si
C18H29F3Si
Organometallics (2003) 22, 20 4136-4144
a=10.8296(16)Å b=10.1669(15)Å c=16.755(3)Å
α=90.0000(10)° β=92.497(3)° γ=90.0000(10)°
C19H32F2Si
C19H32F2Si
Organometallics (2003) 22, 20 4136-4144
a=11.1825(11)Å b=18.9678(19)Å c=17.7010(17)Å
α=90.00° β=90.00° γ=90.00°
C36H49F3Si
C36H49F3Si
Organometallics (2003) 22, 20 4136-4144
a=10.9519(11)Å b=12.0840(12)Å c=25.473(3)Å
α=90.0000(10)° β=90.0000(10)° γ=90.0000(10)°
C47H74F2LiO2PSi2
C47H74F2LiO2PSi2
Organometallics (2003) 22, 20 4136-4144
a=35.59(3)Å b=11.096(10)Å c=25.75(2)Å
α=90.0000(10)° β=96.492(17)° γ=90.0000(10)°
C42H55FNSi
C42H55FNSi
Organometallics (2003) 22, 20 4136-4144
a=13.9095(17)Å b=15.979(2)Å c=17.970(2)Å
α=90.0000(10)° β=109.335(2)° γ=90.0000(10)°
C18H25.5F0.76I0.14Si0.36
C18H25.5F0.76I0.14Si0.36
Organometallics (2003) 22, 20 4136-4144
a=10.9666(10)Å b=12.1283(10)Å c=25.463(2)Å
α=90.0000(10)° β=90.0000(10)° γ=90.0000(10)°
C70H100F4Li2O4P2Si4
C70H100F4Li2O4P2Si4
Organometallics (2003) 22, 20 4136-4144
a=20.973(4)Å b=12.496(3)Å c=27.890(6)Å
α=90.00° β=90.00° γ=90.00°
C33H62F2LiO3PSi2
C33H62F2LiO3PSi2
Organometallics (2003) 22, 20 4136-4144
a=9.0800(11)Å b=10.2208(13)Å c=23.750(3)Å
α=79.227(2)° β=86.878(2)° γ=63.756(2)°
C39H65P2Si3
C39H65P2Si3
Organometallics (2003) 22, 20 4136-4144
a=9.7121(14)Å b=28.021(4)Å c=15.778(2)Å
α=90.0000(10)° β=90.0000(10)° γ=90.0000(10)°
C18H29PSi
C18H29PSi
Organometallics (2003) 22, 20 4136-4144
a=9.2635(10)Å b=9.8504(11)Å c=11.6103(13)Å
α=75.059(3)° β=78.959(3)° γ=65.244(2)°
C18H40Cl2OP2Pd2
C18H40Cl2OP2Pd2
Organometallics (2006) 25, 6 1461-1471
a=15.4000(15)Å b=11.3999(11)Å c=15.4278(15)Å
α=90.00° β=110.881(2)° γ=90.00°
C62H44Cl4F6IrN2OP
C62H44Cl4F6IrN2OP
Organometallics (2006) 25, 6 1461-1471
a=20.4653(19)Å b=12.1974(11)Å c=22.708(2)Å
α=90.00° β=112.026(2)° γ=90.00°
C66H50F6IrN2O3P
C66H50F6IrN2O3P
Organometallics (2006) 25, 6 1461-1471
a=20.579(3)Å b=12.2266(19)Å c=22.819(4)Å
α=90.00° β=113.766(3)° γ=90.00°
C29H15F6N
C29H15F6N
Organometallics (2006) 25, 6 1461-1471
a=17.850(3)Å b=15.742(3)Å c=7.7547(15)Å
α=90.00° β=95.164(5)° γ=90.00°
C80H73F12IrN2O2
C80H73F12IrN2O2
Organometallics (2006) 25, 6 1461-1471
a=11.2969(12)Å b=11.3209(11)Å c=25.322(3)Å
α=87.237(2)° β=87.976(2)° γ=80.299(2)°
C12H10ClN
C12H10ClN
Organometallics (2006) 25, 6 1461-1471
a=7.4452(10)Å b=10.9266(15)Å c=12.0699(16)Å
α=90.00° β=90.00° γ=90.00°
C24H26BrPPd
C24H26BrPPd
Organometallics (2006) 25, 6 1461-1471
a=12.327(3)Å b=12.964(3)Å c=16.075(2)Å
α=90.00° β=108.464(13)° γ=90.00°
C24H27P
C24H27P
Organometallics (2006) 25, 6 1461-1471
a=16.865(10)Å b=8.172(5)Å c=14.598(9)Å
α=90.00° β=103.052(12)° γ=90.00°
C28H19N
C28H19N
Organometallics (2006) 25, 6 1461-1471
a=9.345(4)Å b=7.429(3)Å c=27.666(11)Å
α=90.00° β=107.310(15)° γ=90.00°
C67H55IrN2O2
C67H55IrN2O2
Organometallics (2006) 25, 6 1461-1471
a=25.909(3)Å b=25.909(3)Å c=18.352(4)Å
α=90.00° β=90.00° γ=90.00°
C33H57O0P3
C33H57O0P3
Organometallics (2009) 28, 8 2410
a=9.547(5)Å b=18.178(8)Å c=10.896(5)Å
α=90.00° β=107.703(7)° γ=90.00°
C25H47OPSi
C25H47OPSi
Organometallics (2009) 28, 8 2410
a=9.967(3)Å b=16.096(4)Å c=17.642(5)Å
α=76.105(4)° β=83.726(4)° γ=88.972(4)°
C22H38OP2
C22H38OP2
Organometallics (2009) 28, 8 2410
a=8.6418(19)Å b=11.629(3)Å c=12.587(3)Å
α=90.00° β=108.373(3)° γ=90.00°
C28H56O2Si2
C28H56O2Si2
Organometallics (2009) 28, 8 2410
a=11.1445(12)Å b=11.1579(12)Å c=13.2541(15)Å
α=72.446(2)° β=83.038(2)° γ=85.121(2)°
C186H354Cs6O19P18Si2
C186H354Cs6O19P18Si2
Organometallics (2009) 28, 8 2410
a=28.028(3)Å b=28.028(3)Å c=25.567(4)Å
α=90.00° β=90.00° γ=120.00°
C33H58.5P3
C33H58.5P3
Organometallics (2009) 28, 8 2410
a=9.664(4)Å b=12.213(4)Å c=16.533(6)Å
α=73.253(6)° β=88.408(6)° γ=67.193(5)°
C98H138Cs4N8P4
C98H138Cs4N8P4
Organometallics (2010) 29, 18 4154
a=31.865(3)Å b=24.225(2)Å c=29.185(2)Å
α=90.00° β=112.1930(10)° γ=90.00°
C19H28N
C19H28N
Organometallics (2010) 29, 18 4154
a=16.888(10)Å b=11.023(7)Å c=9.623(6)Å
α=90.00° β=90.00° γ=90.00°
C103H172Cs3N4O7P5
C103H172Cs3N4O7P5
Organometallics (2010) 29, 18 4154
a=60.210(8)Å b=10.9354(16)Å c=35.649(4)Å
α=90.00° β=107.523(3)° γ=90.00°
C128H220Cs2N4O26P6
C128H220Cs2N4O26P6
Organometallics (2010) 29, 18 4154
a=14.607(4)Å b=21.454(6)Å c=23.662(7)Å
α=92.847(7)° β=91.262(7)° γ=103.893(7)°
C12H21F6OP
C12H21F6OP
Organometallics (2004) 23, 25 6031-6041
a=9.0820(10)Å b=11.1281(10)Å c=8.7645(10)Å
α=100.75(2)° β=113.690(10)° γ=69.830(10)°
C12H20F6Ir0.5OP
C12H20F6Ir0.5OP
Organometallics (2004) 23, 25 6031-6041
a=11.2296(17)Å b=9.6565(14)Å c=14.819(2)Å
α=90.00° β=106.727(2)° γ=90.00°
C12H20.5F6Ir0.5OP
C12H20.5F6Ir0.5OP
Organometallics (2004) 23, 25 6031-6041
a=11.2311(19)Å b=9.6227(17)Å c=14.919(3)Å
α=90.00° β=107.020(4)° γ=90.00°
C24H43F12IrO2P2
C24H43F12IrO2P2
Organometallics (2004) 23, 25 6031-6041
a=9.4912(8)Å b=21.647(2)Å c=15.9761(15)Å
α=90.00° β=105.1486(19)° γ=90.00°
C32H41F12IrNO2P
C32H41F12IrNO2P
Organometallics (2004) 23, 25 6031-6041
a=9.4579(8)Å b=13.6204(12)Å c=14.8067(13)Å
α=73.9130(15)° β=74.5780(15)° γ=84.4410(15)°
C33H30ClF12IrN2O2
C33H30ClF12IrN2O2
Organometallics (2004) 23, 25 6031-6041
a=10.8837(15)Å b=11.9141(16)Å c=13.6025(18)Å
α=100.636(3)° β=98.217(3)° γ=94.766(3)°
C12.5H12.5F6Ir0.5O1.5P
C12.5H12.5F6Ir0.5O1.5P
Organometallics (2004) 23, 25 6031-6041
a=9.043(4)Å b=9.584(4)Å c=10.967(5)Å
α=83.273(7)° β=70.193(7)° γ=64.639(7)°
C39H65F12IrN2O3.5P2
C39H65F12IrN2O3.5P2
Organometallics (2004) 23, 25 6031-6041
a=22.181(8)Å b=19.728(7)Å c=21.614(7)Å
α=90.00° β=105.500(6)° γ=90.00°
C25H41F12IrO3P2
C25H41F12IrO3P2
Organometallics (2004) 23, 25 6031-6041
a=8.9000(8)Å b=12.8523(12)Å c=27.710(3)Å
α=90.00° β=91.7441(19)° γ=90.00°
C24H39F12IrO2P2
C24H39F12IrO2P2
Organometallics (2004) 23, 25 6031-6041
a=8.8560(9)Å b=9.3124(9)Å c=11.1189(11)Å
α=65.715(2)° β=75.941(2)° γ=65.218(2)°
C25H39F12IrO3P2
C25H39F12IrO3P2
Organometallics (2004) 23, 25 6031-6041
a=9.9034(8)Å b=11.1101(9)Å c=15.6891(13)Å
α=72.223(2)° β=89.903(2)° γ=73.369(2)°
C40H60F24Ir2O10P4
C40H60F24Ir2O10P4
Organometallics (2004) 23, 25 6031-6041
a=15.111(4)Å b=12.496(4)Å c=15.398(4)Å
α=90.00° β=98.374(5)° γ=90.00°
C30H49IrO4P2
C30H49IrO4P2
Organometallics (2004) 23, 25 6031-6041
a=8.1966(8)Å b=8.6598(9)Å c=12.0745(12)Å
α=78.0812(16)° β=88.8327(17)° γ=69.7442(15)°
C36H60IrO4P2
C36H60IrO4P2
Organometallics (2004) 23, 25 6031-6041
a=12.3338(11)Å b=21.523(2)Å c=14.1769(13)Å
α=90.00° β=97.324(2)° γ=90.00°
C18H29Ir0.5O3P
C18H29Ir0.5O3P
Organometallics (2004) 23, 25 6031-6041
a=9.0060(10)Å b=12.0664(13)Å c=17.0127(19)Å
α=90.00° β=100.517(2)° γ=90.00°
C12H22F3OP
C12H22F3OP
Journal of the American Chemical Society (2007) 129, 9210-9215
a=8.496(3)Å b=20.619(7)Å c=8.291(3)Å
α=90.00° β=102.946(5)° γ=90.00°
C30H55F12IO3P2
C30H55F12IO3P2
Journal of the American Chemical Society (2007) 129, 9210-9215
a=30.271(4)Å b=9.6309(11)Å c=14.2728(17)Å
α=90.00° β=106.203(3)° γ=90.00°
C13H24F6IOP
C13H24F6IOP
Journal of the American Chemical Society (2007) 129, 9210-9215
a=17.242(3)Å b=13.711(2)Å c=17.917(3)Å
α=90.00° β=117.952(2)° γ=90.00°
C14H27F6O2P
C14H27F6O2P
Journal of the American Chemical Society (2007) 129, 9210-9215
a=8.693(2)Å b=23.126(6)Å c=9.831(3)Å
α=90.00° β=114.995(5)° γ=90.00°
C11H19F6INOP
C11H19F6INOP
Journal of the American Chemical Society (2007) 129, 9210-9215
a=31.237(9)Å b=50.033(14)Å c=9.128(3)Å
α=90.00° β=90.00° γ=90.00°
C28H30ClIrN2
C28H30ClIrN2
Inorganic Chemistry (2005) 44, 6244-6247
a=7.9608(15)Å b=18.256(4)Å c=16.595(3)Å
α=90.00° β=98.900(3)° γ=90.00°
C42H38F6IrNOP2
C42H38F6IrNOP2
Inorganic Chemistry (2005) 44, 6244-6247
a=10.9554(11)Å b=17.2237(17)Å c=20.213(2)Å
α=90.00° β=96.322(2)° γ=90.00°
C24H26
C24H26
Organometallics (2003) 22, 20 4136-4144
a=9.0526(13)Å b=11.7904(14)Å c=18.551(3)Å
α=98.155(4)° β=95.820(2)° γ=106.658(3)°
C30H47ClIrO4P2
C30H47ClIrO4P2
Organometallics (2004) 23, 25 6031-6041
a=9.7988(11)Å b=12.3642(14)Å c=26.219(3)Å
α=90.00° β=94.735(2)° γ=90.00°
C10.86H16.86P0.86
C10.86H16.86P0.86
Organometallics (2008) 27, 19 5118
a=11.9102(14)Å b=20.915(2)Å c=15.2058(17)Å
α=90.00° β=104.396(2)° γ=90.00°
C39H61P3
C39H61P3
Organometallics (2008) 27, 19 5118
a=21.285(4)Å b=12.164(2)Å c=29.355(5)Å
α=90.00° β=90.00° γ=90.00°
C45H65P3
C45H65P3
Organometallics (2008) 27, 19 5118
a=13.659(5)Å b=11.857(5)Å c=25.308(14)Å
α=90.00° β=90.00° γ=90.00°
C45H65P3S4
C45H65P3S4
Organometallics (2008) 27, 19 5118
a=38.650(9)Å b=11.962(3)Å c=39.259(15)Å
α=90.00° β=92.036(3)° γ=90.00°
C18H40Cl2OP2Pd2
C18H40Cl2OP2Pd2
Organometallics (2006) 25, 6 1461-1471
a=15.4000(15)Å b=11.3999(11)Å c=15.4278(15)Å
α=90.00° β=110.881(2)° γ=90.00°
C62H44Cl4F6IrN2OP
C62H44Cl4F6IrN2OP
Organometallics (2006) 25, 6 1461-1471
a=20.4653(19)Å b=12.1974(11)Å c=22.708(2)Å
α=90.00° β=112.026(2)° γ=90.00°
C66H50F6IrN2O3P
C66H50F6IrN2O3P
Organometallics (2006) 25, 6 1461-1471
a=20.579(3)Å b=12.2266(19)Å c=22.819(4)Å
α=90.00° β=113.766(3)° γ=90.00°
C12H10ClN
C12H10ClN
Organometallics (2006) 25, 6 1461-1471
a=7.4452(10)Å b=10.9266(15)Å c=12.0699(16)Å
α=90.00° β=90.00° γ=90.00°
C80H73F12IrN2O2
C80H73F12IrN2O2
Organometallics (2006) 25, 6 1461-1471
a=11.2969(12)Å b=11.3209(11)Å c=25.322(3)Å
α=87.237(2)° β=87.976(2)° γ=80.299(2)°
C28H19N
C28H19N
Organometallics (2006) 25, 6 1461-1471
a=9.345(4)Å b=7.429(3)Å c=27.666(11)Å
α=90.00° β=107.310(15)° γ=90.00°
C67H55IrN2O2
C67H55IrN2O2
Organometallics (2006) 25, 6 1461-1471
a=25.909(3)Å b=25.909(3)Å c=18.352(4)Å
α=90.00° β=90.00° γ=90.00°
C24H25Cl4FeN3
C24H25Cl4FeN3
Organometallics (2006) 25, 12 2978
a=10.4140(5)Å b=15.2465(8)Å c=15.8488(8)Å
α=90.00° β=92.3650(10)° γ=90.00°
C94H70Cl4F8Fe2N6
C94H70Cl4F8Fe2N6
Organometallics (2006) 25, 12 2978
a=13.482(5)Å b=23.751(8)Å c=26.066(11)Å
α=90.00° β=90.00° γ=90.00°
C39H27F12N3
C39H27F12N3
Organometallics (2006) 25, 12 2978
a=16.770(2)Å b=15.807(2)Å c=27.350(4)Å
α=90.00° β=90.00° γ=90.00°
C41H31Cl6F12FeN3
C41H31Cl6F12FeN3
Organometallics (2006) 25, 12 2978
a=11.5071(4)Å b=12.4346(5)Å c=31.4986(13)Å
α=90.00° β=100.3450(10)° γ=90.00°
C51H39Cl3F12FeN3
C51H39Cl3F12FeN3
Organometallics (2006) 25, 12 2978
a=16.000(2)Å b=19.310(3)Å c=16.689(3)Å
α=90.00° β=90.168(3)° γ=90.00°
C39H27Cl2F12FeN3
C39H27Cl2F12FeN3
Organometallics (2006) 25, 12 2978
a=32.663(4)Å b=15.197(2)Å c=15.494(2)Å
α=90.00° β=96.197(2)° γ=90.00°
C51H37Cl8F18FeN3
C51H37Cl8F18FeN3
Organometallics (2006) 25, 12 2978
a=20.024(11)Å b=21.142(12)Å c=29.448(18)Å
α=90.00° β=105.241(14)° γ=90.00°
C24H25Cl4FeN3
C24H25Cl4FeN3
Organometallics (2008) 27, 8 1902
a=10.4140(5)Å b=15.2465(8)Å c=15.8488(8)Å
α=90.00° β=92.3650(10)° γ=90.00°
C37H47B2Cl2FeN5O4
C37H47B2Cl2FeN5O4
Organometallics (2008) 27, 8 1902
a=12.6115(19)Å b=16.284(2)Å c=19.867(3)Å
α=90.00° β=104.933(3)° γ=90.00°
C36H42BCl2FeN3O2
C36H42BCl2FeN3O2
Organometallics (2008) 27, 8 1902
a=8.65(2)Å b=23.25(6)Å c=17.26(4)Å
α=90.00° β=90.99(4)° γ=90.00°
C61H74B2Cl6Fe2N6O4
C61H74B2Cl6Fe2N6O4
Organometallics (2008) 27, 8 1902
a=31.466(3)Å b=8.8961(9)Å c=25.037(3)Å
α=90.00° β=111.985(2)° γ=90.00°
C29H33BBrCl2FeN3O2
C29H33BBrCl2FeN3O2
Organometallics (2008) 27, 8 1902
a=14.112(14)Å b=15.854(17)Å c=13.830(15)Å
α=90.00° β=100.75(2)° γ=90.00°
C30H36BCl2FeN3O2
C30H36BCl2FeN3O2
Organometallics (2008) 27, 8 1902
a=14.116(4)Å b=15.902(5)Å c=14.105(4)Å
α=90.00° β=101.311(5)° γ=90.00°
C24H23Cl4F2FeN3
C24H23Cl4F2FeN3
Organometallics (2008) 27, 6 1147
a=15.867(5)Å b=15.220(5)Å c=21.709(7)Å
α=90.00° β=93.565(6)° γ=90.00°
C24H25Cl4FeN3
C24H25Cl4FeN3
Organometallics (2008) 27, 6 1147
a=10.4140(5)Å b=15.2465(8)Å c=15.8488(8)Å
α=90.00° β=92.3650(10)° γ=90.00°
C24H24Cl4FFeN3
C24H24Cl4FFeN3
Organometallics (2008) 27, 6 1147
a=25.6657(10)Å b=15.2699(6)Å c=15.7230(6)Å
α=90.00° β=122.9210(10)° γ=90.00°